A three-dimensional X-ray analysis shows that the co-ordination polyhedron of the five-co-ordinate complex [Ni(tda)I]I is a regular trigonal-bipyramid, unlike that of the analogous complex of CoII which is a square-pyramid.
P. Dapporto and L. Sacconi, J. Chem. Soc. D, 1969, 1091b DOI: 10.1039/C2969001091B
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