Pyrolysis of tetrafluorosuccinic anhydride over potassium fluoride at 410° gives trifluoroacryloyl fluoride in 95% yield. Lower yields of the acryloyl fluoride are obtained by the pyrolysis of tetrafluorosuccinc anhydride over an inert surface and by the pyrolysis of disodium tetrafluorosuccinate.
R. E. Banks, J. M. Birchall, T. Clarke, R. N. Haszeldine, M. J. Stevenson and H. Iserson, J. Chem. Soc. C, 1968, 266 DOI: 10.1039/J39680000266
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