2,2,2-Triphenyl-1,2-oxaphosph(V)olan has been prepared from 3-hydroxypropyltriphenylphosphonium iodide, and rearranges at 300° to 3-phenoxypropyldiphenylphosphine. 2,2,2-Triphenyl-1,2-oxa-ars(V)olan has been prepared from the corresponding arsonium salt, and at 160–180° gave triphenylarsine and allyl alcohol. The nuclear magnetic resonance spectra of the title compounds are given.
A. R. Hands and A. J. H. Mercer, J. Chem. Soc. C, 1967, 1099 DOI: 10.1039/J39670001099
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