The modification of a thermogravimetric balance for pyrolysis studies in a controlled atmosphere is described, together with the way in which the apparatus enables gas flow to be measured accurately. The effect of variable flow-rate of the gas on the pyrolysis of calcium oxalate monohydrate under both air and nitrogen atmospheres is presented and discussed.
J. Bassett and J. W. Betts, Analyst, 1967, 92, 653 DOI: 10.1039/AN9679200653
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