Palladium-catalyzed nucleophilic substitution of propargylic esters using alcohols as nucleophiles has been developed, wherein monohydric alcohols allow the formation of trisubstituted 2-alkoxy-1,3-dienes, while the employment of ethylene glycol leads to the synthesis of 1,4-dioxane derivatives through a double substitution process.
S. Lin, H. Jiang, Y. Zhang, L. Jin, S. Zhang and X. Huang, Org. Chem. Front., 2026, Advance Article , DOI: 10.1039/D5QO01350J
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