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Correction: Catalytic asymmetric hydrometallation of cyclobutenes with salicylaldehydes
F. Wieland
Goetzke
a,
Mireia
Sidera
b and
Stephen P.
Fletcher
*a
aDepartment of Chemistry, University of Oxford, 12 Mansfield Road, Oxford, OX1 3TA, UK. E-mail: stephen.fletcher@chem.ox.ac.uk
bVertex Pharmaceuticals (Europe) Ltd, 86–88 Jubilee Avenue, Milton Park, Abingdon, OX14 4RW, UK
First published on 12th January 2022
Abstract
Correction for ‘Catalytic asymmetric hydrometallation of cyclobutenes with salicylaldehydes’ by F. Wieland Goetzke et al., Chem. Sci., 2022, DOI: 10.1039/d1sc06035j.
The authors regret that the absolute stereochemistry in Scheme 1 presented in the original manuscript was incorrect. The correct version of Scheme 1 is shown below.
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| Scheme 1 Asymmetric hydroacylation of cyclobutenes with different salicylaldehydes.a a[Rh(cod)OH]2 (2.5 mol%), MeDuphos (6 mol%), cyclobutene 2 (0.6 mmol), salicylaldehyde 1 (0.4 mmol), PhMe (0.2 M), 1–4 h. bIncreased catalyst loading of [Rh(cod)OH]2 (5 mol%) and MeDuphos (12 mol%). cDiastereomeric ratios of the unpurified reaction mixtures determined by 1H NMR spectroscopy. All yields refer to isolated yields of the major trans–cis diastereomer. Enantiomeric excesses determined by SFC analysis on a chiral non-racemic stationary phase. | ||
The Royal Society of Chemistry apologises for these errors and any consequent inconvenience to authors and readers.
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