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Abstract | Cited by

Pd-catalyzed alkenylations of metallocenes via C–H activation were developed using electronically tunable pyrazolonaphthyridine (PzNPy) ligands. Ferrocene was alkenylated using the most electron-deficient ligand in the series, whereas the less reactive ruthenocene needed balancing of the electrophilicity and stability of catalysts. Various alkenes were installed, allowing fine-tuning of redox potentials.

Graphical abstract: Nondirected Pd-catalyzed aerobic C–H alkenylation of ruthenocene and ferrocene

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