PEG-grafted nitrogen ligands were synthesized. The corresponding copper complexes serve as metallomicellar nanoreactors for the aerobic tandem desilylation/Glaser coupling of TMS-protected alkynes in water. The protocol is also suitable for base-free homocoupling of terminal alkynes. The metallomicellar catalyst could be recycled 5 times with minor loss of reactivity.
S. Tang, L. Li, X. Ren, J. Li, G. Yang, H. Li and B. Yuan, Green Chem., 2019, 21, 2899 DOI: 10.1039/C8GC03815E
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