Teng
Zhang
,
Weiwei
Liang
,
Yuxing
Huang
,
Xingrong
Li
,
Yizhen
Liu
,
Bo
Yang
,
Chuanxin
He
,
Xuechang
Zhou
and
Junmin
Zhang
*
College of Chemistry and Environmental Engineering, Shenzhen University, Shenzhen, 518060, P. R. China. E-mail: zhangjm@szu.edu.cn
First published on 28th August 2018
Correction for 'Bifunctional organic sponge photocatalyst for efficient cross-dehydrogenative coupling of tertiary amines to ketones' by Teng Zhang et al., Chem. Commun., 2017, 53, 12536–12539.
Entry | x | Solvent | Yieldb (%) |
---|---|---|---|
a Reactions were performed using 1a (0.1 mmol) and 2a (1.0 mmol) in 2 mL of solvent and were catalyzed by sponge catalyst A-7 at room temperature with a 12 W green LED light for 24 hours. b Yield was determined by 1H NMR with 1,3,5-trimethoxybenzene as an internal standard. c <2% ee, determined by chiral HPLC analysis on an AS-H column. d Isolated yield; 7.4% ee. e The yield in the absence of LED irradiation. f The yield in the dark. | |||
1 | 2 | THF | Trace |
2 | 2 | Toluene | Trace |
3 | 2 | DCM | Trace |
4 | 2 | EA | 9 |
5 | 2 | Dioxane | 6 |
6 | 2 | EtOH | 15 |
7 | 2 | NMP | Trace |
8 | 2 | DMF | 18 |
9 | 2 | ACN | 12 |
10 | 2 | DMSO | Trace |
11 | 2 | 2-Methyl-2-pentanol | 30c |
12 | 2 | H 2 O | 81 |
13 | 1.5 | H2O | 72 |
14 | 3 | H 2 O | 95 (93 , 36 , 11 ) |
The Royal Society of Chemistry apologises for these errors and any consequent inconvenience to authors and readers.
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