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Abstract | Cited by

A regio- and stereoselective one-pot C–H insertion/olefination protocol has been developed for the late stage installation of α-methylene-γ-butyrolactones into conformationally restricted cyclohexanol-derivatives. The method has been successfully applied in the total synthesis of eudesmanolide natural product frameworks, including α-cyclocostunolide.

Graphical abstract: A selective C–H insertion/olefination protocol for the synthesis of α-methylene-γ-butyrolactone natural products

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