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Correction: Assessing dimerisation degree and cooperativity in a biomimetic small-molecule model by pulsed EPR
K.
Ackermann
,
A.
Giannoulis
,
D. B.
Cordes
,
A. M. Z.
Slawin
and
B. E.
Bode
*
EaStCHEM School of Chemistry, Biomedical Sciences Research Complex and Centre of Magnetic Resonance, University of St Andrews, North Haugh, St Andrews KY16 9ST, UK. E-mail: beb2@st-andrews.ac.uk
First published on 29th September 2015
Abstract
Correction for ‘Assessing dimerisation degree and cooperativity in a biomimetic small-molecule model by pulsed EPR’ by K. Ackermann et al., Chem. Commun., 2015, 51, 5257–5260.
A mistake was found in the structure of compound 3 in Fig. 1 of the original manuscript. After a revised refinement was carried out, the correct structure of compound 3 was found to be that given in Fig. 1 below.
 | ||
| Fig. 1 Crystal structures of compounds 1 (top) and 3 (bottom). Displacement ellipsoids are drawn at 50% probability; hydrogen atoms, solvent molecules, and minor components of the disorder are omitted for clarity. | ||
The corrected crystal structure experimental details of compound 3 are:
B. Intensity Measurements
Detector Position: 32.59 mm
C. Structure Solution and Refinement
Residuals: R1 (I > 2.00σ(I)): 0.1295
Residuals: R (All reflections): 0.1574
Residuals: wR2 (All reflections): 0.3843
Goodness of Fit Indicator: 1.521
Max Shift/Error in Final Cycle: 0.001
Minimum Peak in Final Diff. Map: −0.68 e− Å−3
The CCDC file corresponding to compound 3 was updated on 22/9/2015 to reflect this correction.
The authors would like to thank Prof. Helen Stoeckli-Evans for highlighting this error.
The Royal Society of Chemistry apologises for these errors and any consequent inconvenience to authors and readers.
| This journal is © The Royal Society of Chemistry 2015 |