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Tripodal cationic N-donor ligands exhibit sterically controlled self-assembly of tetrahedral M6L4 coordination cages that promote selective anion encapsulation (PF6 > OTf) in the solid state. The described method is a potential template for stepwise assembly of hetero-ligand coordination cages and polymers.

Graphical abstract: Sterically controlled self-assembly of tetrahedral M6L4 cages via cationic N-donor ligands

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