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The ortho-lithiation of one diastereoisomer of 4-tert-butylsulfinyl[2.2]paracyclophane is the key step to the synthesis of a range of 4,5-disubstituted [2.2]paracyclophane derivatives.

Graphical abstract: The synthesis and directed ortho-lithiation of 4-tert-butylsulfinyl[2.2]paracyclophane

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