Issue 2, 2003
From the journal:

Mendeleev Communications

N-Thiophosphorylthiourea containing an aza-18-crown-6 fragment. The crystal structure of bis[N-(N'-diisopropoxythiophosphorylamidothiocarbonyl)-aza-18-crown-6]nickel(II)

Felix D. Sokolov,*a   Nail G. Zabirov,a   Vasiliy V. Brusko,a   Dmitry B. Krivolapovb  and  Igor A. Litvinovb  

* Corresponding authors

a Department of Chemistry, Kazan State University, Kazan, Russian Federation, ul. Kremlevskaya, 18, Kazan', Russian Federation
E-mail: felix.sokolov@ksu.ru

b A.E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Centre of the Russian Academy of Sciences, Kazan, Russian Federation, ul. Akademika Arbuzova, 8, Kazan, Russian Federation

Abstract

N-(N'-Diisopropoxythiophosphorylamidothiocarbonyl)aza-18-crown-6 (HL) was obtained by the reaction of aza-18-crown-6 with diisopropoxythiophosphorylisothiocyanate, and its chelate with NiII was characterised using IR, 1H and 31P NMR spectroscopy and single-crystal X-ray diffraction.

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Article information

DOI
https://doi.org/10.1070/MC2003v013n02ABEH001733
Article type
Paper
Submitted
03 Mar 2003

Mendeleev Commun., 2003,13, 72-73

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N-Thiophosphorylthiourea containing an aza-18-crown-6 fragment. The crystal structure of bis[N-(N'-diisopropoxythiophosphorylamidothiocarbonyl)-aza-18-crown-6]nickel(II)

F. D. Sokolov, N. G. Zabirov, V. V. Brusko, D. B. Krivolapov and I. A. Litvinov, Mendeleev Commun., 2003, 13, 72 DOI: 10.1070/MC2003v013n02ABEH001733

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