Issue 62, 2003
From the journal:

CrystEngComm

Temperature-dependent phase transition in a phenylfluorenol inclusion compound

Mino R. Caira,a   Luigi R. Nassimbeni,*a   Hong Sua  and  Edwin Weberb  

* Corresponding authors

a Department of Chemistry, University of Cape Town, Private Bag, Rondebosch, South Africa
E-mail: xrayluig@science.uct.ac.za
Fax: +27 21 6854580
Tel: +27 21 6502569

b Institut für Organische Chemie, Technische Universität Bergakademie Freiberg, Leipziger Strasse 29, Freiberg/Sachs., Germany

Abstract

The inclusion compound 9-phenylfluoren-9-ol·4-methylcyclohexylamine undergoes a phase transition at 232 K. The transition is second order with no change in volume and is accompanied by small change in the host conformation. The structures were determined at 297 K and 193 K, and their lattice energies were calculated.

Graphical abstract: Temperature-dependent phase transition in a phenylfluorenol inclusion compound

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Article information

DOI
https://doi.org/10.1039/B310202E
Article type
Paper
Submitted
26 Aug 2003
Accepted
10 Sep 2003
First published
23 Sep 2003

CrystEngComm, 2003,5, 351-354

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Temperature-dependent phase transition in a phenylfluorenol inclusion compound

M. R. Caira, L. R. Nassimbeni, H. Su and E. Weber, CrystEngComm, 2003, 5, 351 DOI: 10.1039/B310202E

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