Issue 6, 2002
From the journal:

Mendeleev Communications

Palladium-catalysed 3H-labelling of Neu5AcOMe and spacered 3'-sialyllactose

Valerii P. Shevchenko,*a   Igor Yu. Nagaev,a   Nikolai F. Myasoedov,a   Aleksandr B. Tuzikovb  and  Nicolai V. Bovinb  

* Corresponding authors

a Institute of Molecular Genetics, Russian Academy of Sciences, Moscow, Russian Federation, pl. Kurchatova, Moscow, Russian Federation
E-mail: img@glas.apc.org

b M.M. Shemyakin–Yu.A. Ovchinnikov Institute of Bioorganic Chemistry, Russian Academy of Sciences, Moscow, Russian Federation, ul. Miklukho-Maklaya, 16/10, Moscow, Russian Federation

Abstract

Randomly 3H-substituted Neu5AcαOMe and Neu5Acα2-3Galβ1-4Glc-NHCOCH2NH2 were synthesised from 'cold' components using catalytic solid-phase exchange under the following conditions: tritium gas, Pd/CaCO3, 140–160 °C.

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Article information

DOI
https://doi.org/10.1070/MC2002v012n06ABEH001654
Article type
Paper
Submitted
31 Jul 2002

Mendeleev Commun., 2002,12, 215-216

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Palladium-catalysed 3H-labelling of Neu5AcOMe and spacered 3'-sialyllactose

V. P. Shevchenko, I. Yu. Nagaev, N. F. Myasoedov, A. B. Tuzikov and N. V. Bovin, Mendeleev Commun., 2002, 12, 215 DOI: 10.1070/MC2002v012n06ABEH001654

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