Molten salt synthesis and characterization of non-doped hafnia

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Aziza Benamira, Jean-Pierre Deloume and Bernard Durand


Abstract

The reactivity of hafnium tetrachloride towards the molten NaNO3–KNO3 medium is analyzed by thermogravimetry and XRD. After an investigation of the influence of various reaction parameters, an optimized synthesis procedure of the monoclinic variety of hafnia is proposed. The obtained powders are characterized.


References

  1. G. Tilloca, J. Mater. Sci., 1995, 30, 1884 CrossRef CAS.
  2. K. S. Mazdiyazni, C. T. Lynch and J. S. Smith, J. Am. Ceram. Soc., 1965, 48, 372.
  3. A. Lakhlifi, P. Satre, A. Sebaoun and M. Roubin, Ann. Chim. Fr., 1993, 18, 565 Search PubMed.
  4. K. S. Mazdiyazni and L. M. Brown, J. Am. Ceram. Soc., 1970, 53, 43.
  5. H. Toraya, M. Yoshimura and S. Somiya, J. Am. Ceram. Soc., 1983, 662, 148.
  6. M. Jebrouni, B. Durand and M. Roubin, Ann. Chim. Fr., 1991, 16, 569 Search PubMed.
  7. H. Al-Raihani, B. Durand, F. Chassagneux, D. H. Kerridge and D. Inman, J. Mater. Chem., 1994, 4, 1331 RSC.
  8. Y. Du and D. Inman, J. Mater. Chem., 1995, 5, 1927 RSC.
  9. Y. Du and D. Inman, J. Mater. Sci., 1996, 31, 5505 CrossRef CAS.
  10. M. Jebrouni, B. Durand and M. Roubin, Ann. Chim. Fr., 1992, 17, 143 Search PubMed.
  11. V. Harle, J.-P. Deloume, L. Mosoni, B. Durand, M. Vrinat and M. B. Breysse, Eur. J. Solid State Inorg. Chem., 1994, 31, 197 CAS.
  12. E. Kulikova, J.-P. Deloume, L. Mosoni, B. Durand and M. Vrinat, Eur. J. Solid State Inorg. Chem., 1994, 31, 487 CAS.
  13. Y. Du and D. Inman, J. Mater. Chem., 1996, 6, 1239 RSC.
  14. A. Benamira, PhD Thesis, University Claude Bernard-Lyon 1, 1997.
  15. A. Samdi, T. Grollier-Baron, M. Roubin and B. Durand, Powder Technol., 1991, 66, 237 CrossRef CAS.
  16. D. H. Kerridge and J. Cancela-Ray, J. Inorg. Nucl. Chem., 1975, 37, 2257 CAS.
  17. M. H. Miles and A. N. Fletcher, J. Electroanal. Chem., 1987, 221, 115 CrossRef CAS.
  18. E. Desimoni, F. Palmisano, L. Sabbatini and P. G. Zambonin, Anal. Chem., 1979, 51, 822 CrossRef CAS.
  19. M. A. C. G. Van De Graaf, J. H. H. Termaat and A. J. Burggraaf, Ceramic Powders, ed. P. Vincenzini, Elsevier, Amsterdam, 1983, p. 783 Search PubMed.
  20. M. S. Kaliszewski and A. H. Heuer, J. Am. Ceram. Soc., 1990, 73, 1504 CAS.
  21. D. Grier and G. MacCarthy, North Dakota State University, Fargo, ND: ICCD, 1991.
  22. A. Lakhlifi, M. Taha, P. Satre, Y. Jorand, G. Fantozzi and M. Roubin, Ceram. Int., 1996, 23, 349 CrossRef.
  23. A. Samdi, Th. Grollier Baron, B. Durand and M. Roubin, Ann. Chim. Fr., 1988, 13, 171 Search PubMed.
  24. O. Hunter, Jr., R. W. Scheidecker and S. Tojo, Ceram. Int., 1979, 5, 137.
  25. J. E. Bailey, D. Lewis, Z. M. Librant and L. J. Porter, Trans. J. Br. Ceram. Soc., 1972, 71, 25 Search PubMed.
  26. R. C. Garvie, J. Phys. Chem., 1978, 822, 218 CrossRef.
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