Recent progress in cryochemical synthesis of oxide materials

Abstract

Recently conventional cryochemical processes have been complemented by cryoextraction, cryoprecipitation, cryoimpregnation and freeze casting techniques. Considerably more attention is being paid to colloidal solution processing and the application of sol-gel procedures like ion exchange treatment and hydrolysis of organometallic compounds. New preparation methods for nanopowders of various oxides and metals have been developed while further treatment of cryochemical powders using powder engineering techniques allows the powder grain size to vary from 0.2 to 5-6 µm. Cryochemical methods are also suitable for preparation of various porous media, like porous silica or cryogels with surface areas close to those of aerogels, and for the synthesis of HTSC powders for different applications. Fundamental and applied aspects of cryochemical processing are discussed.

References

1. A. Landsberg and T. T. Campbell, J. Metals, 1965, 856.
2. D. W. Johnson Jr. and F. J. Schnettler, J. Am. Ceram. Soc., 1970, 53, 440.
3. P. K. Gallagher and F. Schrey, Thermochim. Acta., 1970, 1, 465.
4. Yu. D. Tretyakov, N. N. Oleynikov and O. A. Shlyakhtin, Cryochemical Processing of Advanced Materials, Chapman & Hall, London, 1997.
5. O. A. Shlyakhtin, A. B. Kulakov, Yu. V. Badun, A. M. Tesker and A. P. Mozhaev, Trans. Mater. Res. Soc. Jpn. A, 1994, 14, 7.
6. H. L. Chang and I. K. Lloyd, J. Am. Ceram. Soc., 1993, 76, 1357.
7. C.-T. Wang, L.-S. Lin and S. J. Yang, J. Am. Ceram. Soc., 1992, 75, 2240.
8. K. Nakajima, S. Shimada and M. Inagaki, J. Ceram. Soc. Jpn., 1995, 103, 304.
9. K. Yamashita, K. V. Ramanujachary and M. Greenblatt, Solid State Ionics, 1995, 81, 53.
10. R. W. Schaeffer, J. Macho, R. E. Salomon, G. Myer, J. E. Crow and P. Pernambuco-Wise, J. Supercond., 1991, 4, 365.
11. N. M. Borisova, Z. V. Golubenko, T. G. Kuz'micheva, L. P. Ol'khovik and V. P. Shabatin, J. Magn. Magn. Mater., 1992, 114, 317.
12. L. I. Martynenko, O. A. Shlyakhtin and D. O. Charkin, Inorg. Mater., 1997, 33, 581.
13. F. Yu. Sharikov, Cryochemical synthesis of finely dispersed oxide powders using ion exchange, PhD thesis, Moscow State University, Moscow, 1991.
14. A. A. Vertegel, S. V. Kalinin, N. N. Oleynikov, Yu. G. Metlin and Yu. D. Tretyakov, J. Mater. Res., 1998, 13, 901.
15. S. M. Kudryavtseva, A. A. Vertegel, S. V. Kalinin, N. N. Oleynikov, L. I. Ryabova, L. L. Meshkov, S. N. Nesterenko, M. N. Rumyantseva and A. M. Gaskov, J. Mater. Chem., 1997, 7, 2269.
16. Yu. D. Tretyakov, V. P. Shabatin, V. R. Sokolovskii, V. G. Merkulov and L. N. Tartakovskaya, USSR Pat. no. 4186083/31-02 from 26.01.87.
17. V. P. Shabatin, Venkateshvara Reddy Bommareddy, V. I. Pershin, Yu. D. Tretyakov and P. E. Kazin, USSR Pat. no. 4749380/33 from 17.10.89.
18. J. Laurie, C. M. Bagnall, B. Harris, R. W. Jones, R. G. Cooke, R. S. Russell-Floyd, T. H. Wang and F. W. Hammett, J. Non-Cryst. Solids, 1992, 147–148, 320.
19. Yu. V. Bugoslavsky, I. G. Naumenko, G. A. Emelchenko and A. D. Caplin, in 5th International Workshop on High-Temperature Superconductors and Novel Materials Engineering (MSU-HTSC-V), Moscow State University, Moscow, 1998, W-62.
20. R. Eggenhoffner, A. Tuccio, R. Masini, A. Diaspro, S. Leporatti and R. Rolandi, Supercond. Sci. Technol., 1997, 10, 142.
21. V. V. Ischenko, O. A. Shlyakhtin and N. N. Oleinikov, Inorg. Mater., 1997, 33, 931.
22. J. M. McHale, P. C. McIntyre and N. V. Coppa, J. Mater. Res., 1996, 11, 1199.
23. E. Bermejo, C. Lacour and M. Quarton, J. Mater. Sci. Lett., 1995, 14, 1346.
24. T. G. Kuz'micheva, L. P. Ol'khovik and V. P. Shabatin, IEEE Trans. Magn. Mater., 1995, 31, 800.
25. V. V. Ischenko, O. A. Shlyakhtin, A. L. Vinokurov, H. Altenburg and N. N. Oleinikov, Physica C, 1997, 282–287, 855.
26. V. V. Ischenko, O. A. Shlyakhtin, N. N. Oleinikov, I. S. Sokolov, H. Altenburg and Yu. D. Tretyakov, Dokl. Chem. (Engl. Transl.), 1997, 356, 217.
27. E. Bermejo, T. Dantas, C. Lacour and M. Quarton, Mater. Res. Bull., 1995, 30, 645.
28. E. Bermejo, T. Becue, C. Lacour and M. Quarton, Powder Technol., 1997, 94, 29.
29. G. M. Pajonk, M. Repellin-Lacroix, S. Abouarnadasse, J. Chaouki and D. Klvana, J. Non-Cryst. Solids, 1990, 121, 66.
30. D. Klvana, J. Chaouki, L. Perras and G. Belanger, in Progress in Catalysis, Elsevier, Amsterdam, 1992, pp. 239–246.
31. G. Amato, N. Brunetto and A. Parisini, Thin Solid Films, 1997, 297, 73.
32. K. Shinoda, E. Matsubara, A. Muramatsu and Y. Waseda, Mater. Trans. JIM, 1994, 35, 394.
33. O. A. Shlyakhtin, R. V. Shpanchenko, E. V. Antipov, V. V. Ischenko and A. P. Mozhaev, in First International Conference on Materials Chemistry, University of Aberdeen, Scotland, UK 19–22 June 1993, Aberdeen 1993, p. 119.
34. J. Kirchnerova and D. B. Hibbert, J. Mater. Sci., 1993, 28, 5800.
35. H. Izutsu, P. K. Nair and F. Mizukami, J. Mater. Chem., 1997, 7, 855.
36. V. Yu. Pomjakushin, A. M. Balagurov, M. V. Lobanov, O. G. Dyachenko, E. V. Antipov, A. M. Abakumov, O. I. Lebedev and G. van Tendeloo, in 5th International Workshop on High-Temperature Superconductors and Novel Materials Engineering (MSU-HTSC-V), Moscow State University, Moscow, 1998, F-22.
37. S. M. Johnson, M. T. Gusman and D. J. Rowcliffe, Adv. Ceram. Mater., 1987, 2(3B), 337.
38. V. P. Shabatin, Ya. V. Fomina, Yu. G. Metlin, Yu. D. Tretyakov, V. V. Moshchalkov, A. M. Tesker and A. B. Kulakov, USSR Pat. no. 4244655/31-33 from 12.05.87.
39. L. Z. Avdeev, N. B. Brandt, A. V. Volkozub, A. A. Gippius, I. E. Graboy, A. R. Kaul, L. M. Kovba, L. N. Lykova, V. V. Moshchalkov, I. G. Muttik, O. V. Snigirev, Yu. D. Tretyakov, R. V. Shpanchenko, V. V. Khanin and Ho Hyu Nyan, Pis'ma v Zh. Eksp. Teor. Fiz., 1987, 46(Suppl.), 82.
40. M. V. Elashkin, A. A. Zhukov, V. P. Shabatin, D. A. Komarkov, V. V. Moshchalkov, I. G. Muttik, N. A. Samarin and A. Yu. Galkin, Physica C, 1989, 162–164, 1173.
41. J. Horn, M. Borner, H. C. Semmelhack, B. Lippold, J. Herrmann, M. Wurlitzer, M. Krotzsch, U. Boehnke, F. Schlenkrich and Ch. Freuzel, Solid State Commun., 1991, 79, 483.
42. S. X. Dou, H. K. Liu, M. H. Apperley, K. H. Song and C. C. Sorrell, Supercond. Sci. Technol., 1990, 3, 138.
43. E. M. M'Hamdi and C. Lacour, Ann. Chim. Fr., 1992, 17, 421.
44. A. D. Nikulin, A. K. Shikov and N. E. Khlebova, IEEE Trans. Magn., 1994, 30, 2368.
45. M. Lelovic, P. Krishnaraj, N. G. Eror and U. Balachandran, Physica C, 1995, 242, 246.
46. O. V. Pupysheva, O. A. Shlyakhtin, V. V. Lennikov, V. I. Putlyaev and Yu. D. Tretyakov, Inorg. Mater., 1997, 33, 951.
47. M. E. Zalischansky, V. P. Shabatin and N. S. Kopelev, in Progress in High Temperature Superconductivity, 1989, 22, 183(Beijing International Conf. on High Temperature Superconductivity, Beijing, China, Sept. 4–8, 1989).
48. S. R. Lee, O. A. Shlyakhtin, M.-O. Mun, M.-K. Bae and S.-I. Lee, Supercond. Sci. Technol., 1995, 8, 60.
49. A. J. Markworth, J. Stringer and R. W. Rollins, MRS Bull., 1995, 7, 20.