Synthesis and Structure of 1,3-[5,5′-(1,2-Phenylenedimethylenedithio)bis-(2,3-dihydro-2-oxo-1,3,4-thiadiazol-3-yl)]propane

(Note: The full text of this document is currently only available in the PDF Version )

Nam Sook Cho, Chang Kown Park, Hye Jeong Hwang, Soon II Hong, Jin-gyu Kim and II-Hwan Suh


Abstract

1,3-[5,5′-(1,2-Phenylenedimethylenedithio)bis(2,3-dihydro-2-oxo-1,3,4-thiadiazol-3-yl)]propane is prepared and its structure clearly established from spectroscopic data (IR, 1H and 13C NMR, and mass spectrometry) and X-ray crystallography.


References

  1. B. Dietrich, P. Viout and J.-M. Lehn, Macrocyclic Chemistry: Aspects of Organic and Inorganic Supramolecular Chemistry, VCH, Weinheim, 1993 Search PubMed.
  2. F. Vögle, Supramolecular Chemistry, Wiley, Chichester, 1991 Search PubMed.
  3. N. S. Cho, C. K. Park, H. S. Kim, E. S. Choi and S. K. Kang, Bull. Korean Chem. Soc., 1998, 19, 103 CAS; Chem. Abstr., 1998, 128, 243634 Search PubMed.
  4. (a) S. R. Cooper, Acc. Chem. Res., 1988, 21, 141 CrossRef CAS; (b) A. L. Blake, J. A. Greig., A. J. Holder, T. I. Hyde, A. Taylor and M. Schröder, Angew. Chem., Int. Ed. Engl., 1990, 29, 197 CrossRef; (c) S. R. Cooper, S. C. Rawle, R. Yagbasan and D. J. Watkin, J. Am. Chem. Soc., 1991, 113, 1600 CrossRef CAS; (d) B. De Groot and S. J. Loeb, Inorg. Chem., 1991, 30, 3103 CrossRef CAS; (e) B. Blackwell, S. M. Ngola, H. Peterson, S. Rosenfeld and C. W. Tingle, J. Org. Chem., 1998, 63, 181 CrossRef CAS.
  5. (a) P. Molia, A. Tarraga, C. Gaspar and A. Espinosa, J. Org. Chem., 1994, 59, 3665 CrossRef; (b) P. Molia, A. Espnsa, A. Tarraga, F. H. Cano and Ma. C. Foces-Foces, J. Chem. Soc., Perkin Trans. 1, 1991, 1159 RSC; (c) F. Bottino, U. Chiacchio, F. R. Fronczek and S. Papparlardo, J. Org. Chem., 1989, 54, 2024 CrossRef CAS; (d) S. Papparlardo, F. Bottino and C. Tringali, J. Org. Chem., 1987, 52, 405, 4309; (e) S. Papparlardo, F. Bottino and C. Tringali, Heterocycles, 1984, 22, 1339; (f) F. Bottino and S. Pappalardo, Tetrahedron, 1982, 38, 665 CrossRef CAS.
  6. N. S. Cho, C. K. Park, H. S. Kim, J. G. Oh, I. H. Suh and M. R. Oh, Heteocycles, in press Search PubMed.
  7. G. M. Sheldrick, SHELXS-86, Acta Crystallogr., Sect. A, 1990, 46, 467 CrossRef.
  8. G. M. Sheldrick SHELXL-97, University of Göttingen, Germany 1997.
  9. I. H. Suh, K. J. Kim, G. H. Choo, J. H. Lee, S. H. Choh and M. J. Kim, Acta Crystallogr., Sect. A, 1993, 49, 369 CrossRef.
Click here to see how this site uses Cookies. View our privacy policy here.