A Convenient and Mild Procedure for the Synthesis of Hydrazones and Semicarbazones from Aldehydes or Ketones under Solvent-free Conditions

Abstract

Hydrazone and semicarbazone derivatives are readily prepared from the corresponding aldehydes or ketones, hydrazine derivatives and semicarbazides under solvent-free conditions.

References

1. H. C. Yoa and P. Resnick, J. Org. Chem., 1965, 30, 2832.
2. R. Fusco and F. Sannicolo, J. Org. Chem., 1981, 46, 90.
3. T. Iida and F. C. Chang, J. Org. Chem., 1981, 46, 2786.
4. R. O. Hutchins, C. A. Milewski and B. E. Maryanoff, J. Am. Chem. Soc., 1949, 71, 2804.
5. I. B. Douglass and R. V. Nuton, J. Org. Chem., 1968, 33, 2104.
6. J. H. Youn and R. Herrmann, Synthesis, 1987, 72.
7. G. Barm, A. Loupy, M. Majdoub, E. Gutierrez and E. Ruiz-Hitzky, Tetrahedron, 1990, 46, 5167.
8. A. R. Hajipour, I. Mohammadpoor-Baltork, K. Nikbaghat and H. Imanzadeh, Synth. Commun., 1999, 29, 1697.
9. A. R. Hajipour, S. E. Mallakpour and H. Imanzadeh, J. Chem Res. (S), in press.
10. A. R. Hajipour, S. E. Mallakpour and H. Imanzadeh, Chem Lett, 1999, 99.
11. A. R. Hajipour, Indian J. Chem. Sect. B., 1997, 36, 1069.
12. A. R. Hajipour, S. E. Mallakpour and A. Afrousheh, Tetrahedron, 1999, 55, 231.
13. R. Shriner, R. C. Fuson, D. Y. Curtin and T. C. Morrill, The Identification of Organic Compounds, John Wileyand Sons, New York, 1980, pp. 558–560; G. R. Newkome and D. L. Fishel, J. Org. Chem., 1966, 31, 677.
14. A. R. Hajipour and N. Mahboubghah, Synth. Commun., 1998, 28, 3143.
15. A. R. Hajipour and N. Mahboubghah, Org. Prep. Proc. Int., 1999, 31, 112.