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DOI: 10.1039/A904344F (Paper) Reference Section for: J. Chem. Soc., Dalton Trans., 1999, 2407-2408

Hydroxyethylmethacrylate as a source of ethyleneglycolate ligands. Synthesis and characterization of Nb4(µ,η1,η2-OC2H4O)2(µ3,η1,η2-OC2H4O)2(µ-OC2H4O)(OPri)10

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Liliane G. Hubert-Pfalzgraf, Valérie Abada and Jacqueline Vaissermann

Abstract

The reaction between niobium isopropoxide and 2-hydroxyethylmethacrylate (HEMA) at room temperature (1∶1 stoichiometry) afforded [Nb4(µ,η1,η2-OC2H4O)2(µ3,η1,η2-OC2H4O)2(µ-OC2H4O)(OPri)10] as characterized by X-ray diffraction.

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