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DOI: 10.1039/A806858E (Paper) Reference Section for: J. Chem. Soc., Dalton Trans., 1998, 3987-3990

First structural characterisation of nitro–nitrito linkage isomers of nickel(II): synthesis and single crystal structures of [NiL2(NO2)2] and [NiL2(ONO)2] [L = 1-(2-aminoethyl)piperidine]

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Debasis Das, Inamur Rahaman Laskar, Ashutosh Ghosh, Arunendu Mondal, Ken-ichi Okamoto and Nirmalendu Ray Chaudhuri

Abstract

The linkage isomers trans-bis[1-(2-aminoethyl)piperidine]dinitronickel(II) (brown) 1 and trans-bis[1-(2-aminoethyl)piperidine]dinitritonickel(II) (blue) 2 have been synthesized and characterised by X-ray single crystal structure analysis.

References

  1. M. A. Hitchman and G. L. Rowbottom, Coord. Chem. Rev., 1982, 42, 55 CrossRef CAS.
  2. F. Basolo and G. S. Hammakar, J. Am. Chem. Soc., 1960, 82, 1001 CAS; Inorg. Chem., 1962, 1, 1 Search PubMed.
  3. D. M. L. Goodgame and M. A. Hitchman, Inorg. Chem., 1966, 5, 1303 CrossRef CAS.
  4. R. W. Green and B. Bell, Aust. J. Chem., 1973, 26, 1663 CAS.
  5. R. W. Green, Chem. Commun., 1969, 1463 RSC.
  6. R. W. Green, Aust. J. Chem., 1973, 26, 1841 CAS.
  7. A. J. Finney, M. A. Hitchman, C. L. Raston, G. L. Rowbottom and A. H. White, Aust. J. Chem., 1981, 34, 2061; 2069 CAS.
  8. M. J. Goldberg and R. E. Marsh, Acta Crystallogr., Sect. B, 1979, 35, 960 CrossRef.
  9. D. M. L. Goodgame and M. A. Hitchman, Inorg. Chim. Acta, 1969, 3, 319 CrossRef CAS.
  10. A. I. Vogel, A Text Book of Quantitative Inorganic Analysis, Longman, New York, 4th edn., 1978 Search PubMed.
  11. SIR 92, A. Altomare, M. C. Burla, M. Camalli, M. Cascarano, C. Giacovazzo, A. Guagliardi and G. Polidori, J. Appl. Crystallogr., 1994, 27, 425 Search PubMed.
  12. P. T. Beurskens, G. Admiraal, G. Beurskens, W. P. Bosman, R. de Gelder, R. Israel and J. M. M. Smits, The DIRDIF 94 program system, Technical Report of the Crystallography Laboratory, University of Nijmegen, 1994.
  13. D. T. Cromer and J. T. Waber, International Tables for X-Ray Crystallography, Kynoch press, Birmingham, 1974, vol. 4, Table 2.2 A Search PubMed.
  14. J. A. Ibers and W. C. Hamilton, Acta Crystallogr., 1964, 17, 781 CrossRef.
  15. D. C. Creagh and W. J. McAuley, International Tables for Crystallography, ed. A. J. C. Wilson, Kluwer, Boston, 1992, vol. C, Table 4.2.6.8, p. 219 Search PubMed.
  16. D. C. Creagh and J. H. Hubbell, International Tables for Crystallography, ed. A. J. C. Wilson, Kluwer, Boston, 1992, vol. C, Table 4.2.4.3, p. 200 Search PubMed.
  17. TEXSAN, Crystal Structure Analysis Package, Molecular Structure Corporation, Houston, TX, 1985 and 1992.
  18. R. E. Weston and T. F. Brodasky, J. Chem. Phys., 1957, 27, 683 CrossRef CAS.
  19. J. Chatt, L. A. Duncanson, B. M. Gatehouse, J. Lewis, R. S. Nyholm, M. L. Tobe, P. F. Todd and L. M. Venanzi, J. Chem. Soc., 1959, 4073 RSC.
  20. D. M. L. Goodgame and L. M. Venanzi, J. Chem. Soc., 1963, 616 RSC.
  21. L. El-Sayed and R. O. Ragsdale, Inorg. Chem., 1967, 6, 1640 CrossRef CAS.
  22. K. Nakamoto, J. Fujita and H. Murata, J. Am. Chem. Soc., 1958, 80, 4817 CrossRef CAS.
  23. K. Nakamoto, Infrared Spectra of Inorganic and Coordination Compounds, Wiley, New York, 1977, p. 223 Search PubMed.
  24. G. Blyholder and A. Kittila, J. Phys. Chem., 1963, 67, 2147 CAS.
  25. C. K. Johnson, ORTEP, Report ORNL-5138, Oak Ridge National Laboratory, Oak Ridge, TN, 1976.
  26. A. K. Mukherjee, M. Mukherjee, A. J. Welch, A. Ghosh, G. De and N. Ray Chaudhuri, J. Chem. Soc., Dalton Trans., 1987, 997 RSC.
  27. A. J. Blake, J. P. Danks, S. Parsons and M. Schröder, Acta Crystallogr., Sect. C, 1997, 53, 411 CrossRef.
  28. D. Das, N. P. Nayak, A. K. Mukherjee and N. Ray Chaudhuri, Polyhedron, 1997, 16, 3305 CrossRef CAS.
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