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DOI: 10.1039/A800952J (Paper) Reference Section for: J. Chem. Soc., Dalton Trans., 1998, 875-876

A novel access to ionic superoxides and the first accurate determination of the bond distance in O2–

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Hady Seyeda and Martin Jansen

Abstract

The compound [C6H4(NMe3)2-1,3][O2]2·3NH3 was prepared from [NMe4][O2] via cation-exchange in liquid ammonia; the bond length of the superoxide anion was determined by X-ray crystallographic analysis to be 134(3) pm.

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