View PDF Version
 
DOI: 10.1039/A706950B (Paper) Reference Section for: Chem. Commun., 1998, 117-118

Structure of templated microcrystalline DAF-5† (Co0.28Al0.72PO4C10H20N2) determined by synchrotron-based diffraction methods

(Note: The full text of this document is currently only available in the PDF Version )

Gopinathan Sankar, Joanna K. Wyles, John Meurig Thomas, C. Richard A. Catlow, Dewi W. Lewis, Simon J. Coles, Gopinathan Sankar, Richard H. Jones, Dewi W. Lewis, William Clegg, Simon J. Coles, Simon J. Teat, William Clegg and Simon J. Teat

Abstract

Micro-single crystal diffraction techniques employing synchrotron radiation are used to determine the structures of the disordered template (4-piperidinopiperidine) within the recently synthesised, chabazite-related cobalt aluminium phosphate known as DAF-5; the structural details revealed are inaccessible by high-resolution powder diffraction.

References

  1. I. E. Maxwell and P. W. Lednor, Curr. Op. Solid State Mater. Chem., 1996, 1, 57 Search PubMed.
  2. D. W. Lewis, D. J. Willock, C. R. A. Catlow, J. M. Thomas and G. J. Hutchings, Nature, 1996, 382, 604 CrossRef CAS.
  3. D. J. Willock, D. W. Lewis, C. R. A. Catlow, J. M. Thomas and G. J. Hutchings, J. Mol. Catal. A, in press Search PubMed.
  4. D. W. Lewis, G. Sankar, J. K. Wyles, J. M. Thomas, C. R. A. Catlow and D. J. Willock, Angew. Chem., Int. Ed. Engl., 1997, in press Search PubMed.
  5. P. A. Barrett, R. H. Jones, J. M. Thomas, C. Saukar, I. J. Shannon and C. R. A. Catlow, Chem. Commun., 1996, 2001 RSC.
  6. P. E. Werner, L. Eriksson and M. Westdahl, J. Appl. Crystallogr., 1985, 18, 367 CrossRef CAS.
  7. A. LeBail, H. Duroy and J. L. Fourquet, Mater. Res. Bull., 1988, 23, 447 CrossRef CAS.
  8. C. Giacovazzo, Acta. Crystallogr., Sect. A, 1996, 52, 331 CrossRef.
  9. H. M. Rietveld, J. Appl. Crystallogr., 1969, 2, 65 CrossRef CAS.
  10. A. C. Larson and R. B. von Dreele, GSAS, Report no. LA-UR-86-748, Los Alamos National Library, NM, 1987.
  11. H. E. King, L. A. Mundi, K. G. Strohmaier and R. C. Haushalter, J. Solid State Chem., 1991, 92, 1 CrossRef CAS.
  12. G. W. Noble, P. A. Wright, P. Lightfoot, R. E. Morris, K. J. Hudson, A. Kvick and H. Graafsma, Angew. Chem., Int. Ed. Engl., 1997, 36, 81 CrossRef CAS.
  13. G. Cheetham and M. M. Harding, Zeolites, 1996, 16, 245 CrossRef CAS.
  14. R. J. Cernik, W. Clegg, C. R. A. Catlow, G. Bushell-Wye, J. V. Flaherty, G. N. Greaves, I. D. Burrows, D. J. Taylor, S. J. Teat and M. Hamichi, J. Synchrotron Rad., 1997, in press Search PubMed.
  15. G. M. Sheldrick, SHELXS86 User guide, University of Göttingen, 1986.
  16. Discover v95.0, Molecular Simulations Inc., San Diego, CA, 1996.
Click here to see how this site uses Cookies. View our privacy policy here.