Development and application of an automated gas chromatographic sampling system for verification of test vapor stream concentrations for chemical sensor studies

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Timothy Torkelson and David S. Ballantine


Abstract

An automated GC sampling system is described which permits real-time verification of vapor stream concentrations used in the testing and development of chemical sensors. The system consists of a computer-actuated injector loop placed in-line between a VG-400 vapor generator (Microsensor Systems) and a surface acoustic wave (SAW) sensor. Optimization of the system was performed by comparing the predicted VG-400 vapor output with the GC-determined vapor stream concentrations. The system was utilized in the identification of hystersis effects in a polymer-coated SAW sensor.


References

  1. G. P. Neill, N. W. Davies and S. McLean, J. Chromatogr., 1991, 565, 207 CrossRef CAS.
  2. H. J. Stan and F. Schwarzer, J. Chromatogr. A, 1993, 653, 45 CrossRef CAS.
  3. J. W. Grate, S. Rose-Pehrsson and D. L. Venezky, Anal. Chem., 1993, 65, 1868 CrossRef CAS.
  4. J. J. Szakasits and R. E. Robinson, Anal. Chem., 1991, 63, 114 CrossRef CAS.
  5. C. Filippini, J. U. Moser, B. Sonnleitner and A. Fiechter, Anal. Chim. Acta, 1991, 255, 91 CrossRef CAS.
  6. E. M. Stansbridge, G. A. Mills and V. Walker, J. Chromatogr., 1993, 621, 7 CrossRef CAS.
  7. J. P. Greenberg, B. Lee, D. Helmig and P. R. Simmerman, J. Chromatogr. A, 1994, 676, 389 CrossRef CAS.
  8. J. Gan, S. R. Yates, W. F. Spencer and M. V. Yates, J. Chromatogr. A, 1994, 684, 121 CrossRef CAS.
  9. Y. Youchi, H. Bandow and H. Akimoto, J. Chromatogr., 1993, 642, 401 CrossRef CAS.
  10. R. Annino, J. Chromatogr., 1994, 678, 678 CrossRef CAS.
  11. R. S. Barrat, Analyst, 1981, 106, 817 RSC and references cited therein.
  12. G. O. Nelson, Gas Mixtures: Preparation and Control, Lewis, Chelsea, MI, 1992 Search PubMed.
  13. J. W. Grate and M. Klusty, Naval Research Laboratory Report No. AD-A229, US Government Printing Office, Washington, DC, 1990 Search PubMed.
  14. S. J. Martin and G. C. Frye, Proc. IEEE Ultrason. Symp., 1991, 393 Search PubMed.
  15. S. J. Martin and G. C. Frye, Proc. IEEE Ultrason. Symp., 1992, 27 Search PubMed.
  16. J. W. Grate, M. Klusty, R. A. McGill, M. H. Abraham, G. Whiting and J. Andonian-Haftvan, Anal. Chem., 1992, 64, 610 CrossRef CAS.
  17. D. S. Ballantine, Anal. Chem., 1992, 64, 309.
  18. S. J. Martin, G. C. Frye and S. D. Senturia, Anal. Chem., 1994, 66, 2201 CrossRef CAS.
  19. G. C. Frye and S. J. Martin, Proc. Electrochem. Soc., 1993, 93, 51 Search PubMed.
  20. VG-400 Automatic Vapor Generation System Operating Manual, Microsensor Systems, Bowling Green, KY, 1990 Search PubMed.
  21. CRC Handbook of Chemistry and Physics, ed. Weast, R. C., CRC Press, Cleveland, OH, 52nd edn., 1972, p. D-146 Search PubMed.
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