Effect of nitric acid digestion on organic materials and silica in rice husk

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I. A. Rahman, J. Ismail and H. Osman


Abstract

Studies on the digestion of rice husk by HNO3 at 65 °C over 2–12 h have been carried out. Changes in the physical characteristics and morphology of rice husk due to the degradative effect of nitric acid were studied by using thermogravimetric analysis and scanning electron microscopy. It was observed that the residue obtained after 12 h digestion is a mixture of loose cellulose fibres and fragments of a cellulose–silica composite consisting mainly of cellulose (ca. 24%) and silica (ca. 76%), respectively.


References

  1. Malaysian Agricultural Directory and Index 1993/94, Ministry of Agricultural, Kuala Lumpur, Malaysia.
  2. I. A. Rahman, J. Mater. Chem., 1992, 2, 1107 RSC.
  3. F. Adam, I. A. Rahman and M. I. Saleh, in Seramik Nusantara, ed. R. Othman, U.S.M. Penang, Malaysia, 1990, pp. 261–273 Search PubMed.
  4. M. A. Hamad, J. Chem. Biotechnol., 1981, 31, 624 Search PubMed.
  5. TAPPI T6 revised: T 204 05, 1976.
  6. L. E. Wise, E. J. Murphy and A. A. D'Addieco, Paper Trade J., 1946, 122, 35 Search PubMed.
  7. TAPPI T203, revised: T 203 05, 1974.
  8. I. A. Rahman and F. L. Riley, J. Eur. Ceram. Soc., 1989, 5, 11 CrossRef CAS.
  9. I. A. Rahman, Ceram. Inter., 1994, 20, 195 CrossRef CAS.
  10. I. A. Rahman and M. I. Saleh, Mater. Lett., 1995, 23, 157 CrossRef CAS.
  11. J. G. Lee and I. B. Cuttler, Am. Ceram. Bull., 1975, 54, 195 CAS.
  12. H. Hamdan and E. Listiorini, Buletin Kimia, 1994, 9, 37 Search PubMed.
  13. K. Voshimichi, S. Kumio, S. Tsuneji, M. Fujio and S. Shigenitsu, Chem. Express, 1992, 7, 521 Search PubMed.
  14. S. Tamin and I. Gurgey, Chim. Acta Turc., 1988, 16, 58 Search PubMed.
  15. H. Tanzil, T. Wahab and S. Zafar Ahmad, Pak. J. Sci. Ind. Res., 1988, 31, 221 Search PubMed.
  16. M. Cici and E. Keles, Pak. J. Sci. Ind. Res., 1990, 33, 347 Search PubMed.
  17. I. A. Rahman and J. Ismail, J. Mater. Chem., 1993, 3, 931 RSC.
  18. M. Patel, A. Karera and P. Prasanna, J. Mater. Sci., 1987, 22, 2457 CAS.
  19. W. Schnabel, Polymer Degradation—Principles and Practical Applications, Hanser International, Munich, Germany, 1981, p. 204 Search PubMed.
  20. J. James and M. S. Rao, Thermochim. Acta, 1986, 97, 329 CrossRef CAS.
  21. P. Yang and S. Kokot, J. Appl. Polym. Sci., 1996, 60, 1137 CrossRef CAS.
  22. A. Basch and M. Lewin, J. Polym. Sci., Polym. Chem. Ed., 1974, 12, 2035 CrossRef.
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