Montmorillonite Clay Catalysis. Part 4.1 An Efficient and Convenient Procedure for Preparation of 1,1-Diacetates from Aldehydes

Abstract

An easy preparation of 1,1-diacetates from aldehydes with montmorillonite clays as catalysts has been carried out in excellent yield.

References

1. Part 3: T. S. Li and S. H. Li, Synth. Commun., 1997, in the press.
2. K. S. Kochhar, B. S. Bal, R. P. Deshpande, S. N. Rajadhyaksha and H. W. Pinnick, J. Org. Chem., 1983, 48, 1765.
3. J. Kula, Synth. Commun., 1986, 16, 833.
4. M. J. Gregory, J. Chem. Soc. B, 1970, 1201.
5. E. R. Perez, A. L. Marrero, R. Perez and M. A. Autie, Tetrahedron Lett., 1995, 36, 1779.
6. Y. Y. Ku, R. Patel and D. Sawick, Tetrahedron Lett., 1993, 34, 8037.
7. S. V. Lieberman and R. Connor, Org. Synth., 1951, Coll. Vol. II, 441.
8. B. B. Snider and S. G. Amin, Synth. Commun., 1978, 8, 117.
9. M. Tomita, T. Kikuchi, K. Bessho, T. Hori and Y. Inubushi, Chem. Pharm. Bull., 1963, 11, 1484.
10. F. Freeman and E. M. Karcherski, J. Chem. Eng. Data, 1977, 22, 355.
11. I. Scriabine, Bull. Soc. Chim. Fr., 1961, 1194.
12. J. K. Michie and J. A. Miller, Synthesis, 1981, 824.
13. G. A. Olah and A. K. Mehrotra, Synthesis, 1982, 962.
14. C. Pereira, B. Cigante, M. J. Marcelo-Curto, H. Carreyre, G. Perot and M. Guisnet, Synthesis, 1995, 1077.
15. P. Kumar, V. R. Hegda and T. P. Kumar, Tetrahedron Lett., 1995, 36, 601.
16. S. V. N. Raju, J. Chem. Res. (S), 1996, 68.
17. M. V. Joshi, C. S. Narasimhan and O. Mukesh, J. Catal., 1993, 141, 308.
18. For a recent review see: T. S. Li and T. S. Jin, Chin. J. Org. Chem., 1996, 16, 385.
19. N. S. Vulfson, Zh. Obshch. Khim., 1950, 20, 595 (Chem. Abstr., 1951, 45, 557b).
20. I. Hisashi and T. Seisuke, J. Pharm. Soc. Jpn., 1952, 72, 876 (Chem. Abstr., 1953, 47, 6413b).