Isolation and comprehensive solid state characterization of Cl3Al–O–PCl3

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Neil Burford, Andrew D. Phillips, Robert W. Schurko, Roderick E. Wasylishen and John F. Richardson


Abstract

The crystal structure of Cl3Al–O–PCl3 contains covalent molecular units with an essentially linear Al–O–P axis, and a similar solution structure is indicated by NMR spectroscopy.


References

  1. W. Casselmann, Ann. Chem., 1852, 83, 257 Search PubMed; 1856, 98, 213.
  2. V. Gutmann and M. Z. Baaz, Z. Anorg. Allg. Chem., 1959, 298, 121 CrossRef.
  3. V. Gutmann and M. Z. Baaz, Monatsh. Chem., 1959, 90, 729 CAS.
  4. J. Lewis and D. B. Sowerby, J. Chem. Soc., 1963, 1305 RSC.
  5. F. Birkeneder, R. W. Berg and N. J. Bjerrum, Acta Chem. Scand., 1993, 47, 344 CAS.
  6. R. G. Kidd and D. R. Truax, Chem. Commun., 1969, 160 RSC.
  7. S. Boghosian, G. Zissi and G. A. Voyiatzis, Proc. Electrochem. Soc., 1994, 276 Search PubMed.
  8. A. S. Barabanova and B. A. Voitovich, Russ. J. Inorg. Chem., 1964, 12, 1455.
  9. A. V. Suvorov and V. L. Shubaev, Russ. J. Inorg. Chem., 1971, 16, 166.
  10. L. A. Nisel'son, T. D. Sokolova, Y. N. Lyzlov and S. I. Solov'ev, Russ. J. Inorg. Chem., 1976, 21, 1578.
  11. S. Boghosian, D. A. Karydis and G. A. Voyiatzis, Polyhedron, 1993, 12, 771 CrossRef CAS.
  12. H. Gerding, J. A. Koningstein and E. R. van der Worm, Spectrochim. Acta, 1960, 16, 881 CrossRef CAS.
  13. E. W. Wartenberg and J. Goubeau, Z. Anorg. Allg. Chem., 1964, 329, 269 CrossRef CAS.
  14. V. L. Shubaev, A. V. Suvorov and G. A. Semenov, Russ, J. Inorg. Chem., 1970, 15, 479; A. V. Suvorov, Koord. Khim., 1977, 3, 1469 Search PubMed.
  15. B. A. Voitovich, A. S. Barabanova and G. N. Novitskaya, Ukr. Khim. Z., 1967, 33, 367 Search PubMed.
  16. I. L. Nadelyaeva, Yu. V. Kondrat'ev and A. V. Suvorov, J. Gen. Chem. USSR, 1974, 46, 1413 Search PubMed.
  17. W. L. Groeneveld and A. P. Zurr, Recl. Trav. Chim. Pays-Bas, 1957, 76, 1005 CAS; J. Inorg. Nucl. Chem., 1958, 8, 241 Search PubMed.
  18. See, for example, J. L. Atwood and M. J. Zaworotko, J. Chem. Soc., Chem. Commun., 1983, 302 Search PubMed.
  19. N. Burford, B. W. Royan, R. E. v. H. Spence, T. S. Cameron, A. Linden and R. D. Rogers, J. Chem. Soc., Dalton Trans., 1990, 1521 RSC.
  20. T. Okuda, H. Ishihara, K. Yamada and H. Negita, Bull. Chem. Soc. Jpn., 1978, 51, 1273 CAS.
  21. J. Petersen, E. Lork and R. Mews, Chem. Commun., 1996, 1897 RSC.
  22. N. Burford, Coord. Chem. Rev., 1992, 112, 1 CrossRef CAS.
  23. Y. Kushi and Q. Fernando, J. Am. Chem. Soc., 1970, 92, 91 CrossRef CAS.
  24. C. Glidewell and D. C. Liles, J. Chem. Soc., Chem. Commun., 1977, 632 RSC.
  25. A. Aaberg, T. Gramstad and S. Husebye, Acta Chem. Scand., 1980, 34, 717 Search PubMed.
  26. M. B. Power, S. G. Bott, D. L. Clark, J. L. Atwood and A. R. Barron, Organometallics, 1990, 9, 3086 CrossRef CAS.
  27. R. Steudel, Chemistry of the Non-Metals, de Guyter, New York, 1977 Search PubMed.
  28. W. Airey, C. Glidewell, A. G. Robiette and G. M. Sheldrick, J. Mol. Struct., 1971, 8, 413 CrossRef CAS.
  29. C. Glidewell, Inorg. Chim. Acta, 1975, 12, 219 CrossRef CAS.
  30. R. J. Gillespie and I. Hargittai, The VSEPR Model of Molecular Geometry, Allyn and Bacon, Boston, 1991 Search PubMed; R. J. Gillespie, Chem. Soc. Rev., 1992, 59 Search PubMed.
  31. R. C. Lord, D. W. Robinson and W. C. Schumb, J. Am. Chem. Soc., 1956, 78, 1327 CrossRef CAS; A. Almenningen, O. Bastiansen, V. Ewing, K. Hedberg and M. Treatteberg, Acta Chem. Scand., 1963, 17, 7.
  32. A. H. Mellor and N. C. Mathieson, Acta Crystallogr., 1952, 5, 185 CrossRef.
  33. N. M. Karayannis, C. K. Mikulski and L. L. Pytlewski, Inorg. Chim. Acta Rev., 1971, 5, 69 Search PubMed; M. W. G. de Bolster, Top. Phosphorus Chem., 1983, 11, 69 Search PubMed.
  34. G. Munninghoff, E. Hellner, M. El Essawi and K. Dehnicke, Z. Kristallogr., 1978, 147, 231.
  35. T. Moritani, K. Kuchitsu and Y. Morino, Inorg. Chem., 1971, 10, 344 CrossRef.
  36. T. J. LePage and K. B. Wiberg, J. Am. Chem. Soc., 1988, 110, 6642 CrossRef CAS.
  37. S. Boghosian, G. A. Voyiatzis and G. N. Papatheodorou, J. Chem. Soc., Dalton Trans., 1996, 3405 RSC.
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