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DOI: 10.1039/A705053D (Paper) Reference Section for: Chem. Commun., 1997, 2045-2046

Application of triple-channel 13C{1H,19F} NMR techniques to probe structural properties of disordered solids

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Alison Nordon, Robin K. Harris, Alison Nordon, Lily Yeo and Kenneth D. M. Harris

Abstract

Triple-channel 13C MAS NMR experiments are carried out to characterize intermolecular interactions in disordered molecular solids containing fluorinated n-alkanes; an approach involving a combination of 1H→13C and 19F→13C cross-polarization experiments, with both single-channel (1H) and double-channel (1H,19F) decoupling is developed to assign resonances for a given type of 13C nucleus in different intermolecular environments.

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