Thioether macrocycles as spacers for crystal engineering: synthesis and crystal structures of [Ag2([24]aneS8)(CF3SO3)2(MeCN)2] and [Ag([16]aneS4)(BF4)]([24]aneS8 = 1,4,7,10,13,16,19,22-octathiacyclotetracosane; [16]aneS4 = 1,5,9,13-tetrathiacyclohexadecane)

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Alexander J. Blake and Martin Schröder


Abstract

The polymeric complexes [Ag2([24]aneS8)(CF3SO3)2- (MeCN)2] and [Ag([16]aneS4)(BF4)] show infinite ladder and layered structures respectively, with the thioether crown controlling the multi-dimensional architecture.


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