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DOI: 10.1039/A701253E (Paper) Reference Section for: Chem. Commun., 1997, 867-868

Hydro(solvo)thermal synthesis and structure of a three-dimensional zinc fluorophosphate: Zn2(4,4′-bipy)(PO3F)2

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P. Shiv Halasyamani, Mark J. Drewitt and Dermot O’Hare

Abstract

A new three-dimensional zinc fluorophosphate is prepared by using hydro(solvo)thermal conditions with ZnO, (HF)x·py H3PO4 and 4,4′-bipyridyl; the single-crystal structure is determined.

References

  1. M. E. Davis and R. F. Lobo, Chem. Mater., 1992, 4, 756 CrossRef CAS.
  2. D. W. Breck, Zeolite Molecule Sieves: Structure, Chemistry and Use, Wiley, 1974 Search PubMed.
  3. P. B. Venuto, Microporous Mater., 1994, 2, 297 CrossRef CAS.
  4. R. C. Haushalter and L. A. Mundi, Chem. Mater., 1992, 4, 31 CrossRef CAS.
  5. T. E. Gier and G. D. Stucky, Nature, 1991, 349, 508 CrossRef CAS.
  6. W. T. A. Harrison and M. L. F. Phillips, Chem. Commun., 1996, 2771 RSC.
  7. R. M. Barrier, Hydrothermal Chemistry of Zeolites, Academic Press, 1982 Search PubMed.
  8. R. Szostak, Molecular Sieves: Principles of Synthesis and Identification, Van Nostrand Reinhold, 1989 Search PubMed.
  9. P. Halasyamani, M. J. Willis, C. L. Stern, P. Lundquist, H. G. Wong and K. R. Poeppelmeier, Inorg. Chem., 1996, 35, 1367 CrossRef CAS.
  10. P. Halasyamani, K. R. Heier, M. J. Willis, C. L. Stern and K. R. Poeppelmeier, Z. Anorg. Allg. Chem., 1996, 622, 479 CrossRef CAS.
  11. P. Halasyamani, K. R. Heier, C. L. Stern and K. R. Poeppelmeier, manuscript in preparation.
  12. G. Ferey, J. Fluorine Chem., 1995, 72, 187 CrossRef CAS and references therein.
  13. M. Berraho, C. R'Kha, A. Vegas and M. Rafiq, Acta Crystallogr., Sect. C, 1992, 48, 1350 CrossRef.
  14. A. F. Berndt, Acta Crystallogr., Sect. B, 1974, 30, 529 CrossRef.
  15. J. Durand, L. Cot, M. Berraho and M. Rafiq, Acta Crystallogr., Sect. C, 1987, 43, 611 CrossRef.
  16. M. Zeibig, B. Wallis, F. Mowius and M. Meisel, Z. Anorg. Allg. Chem., 1991, 600, 231 CrossRef CAS.
  17. P. J. Durand, A. Larbot, L. Cot, M. Duprat and F. Dabosi, Z. Anorg. Allg. Chem., 1983, 504, 163 CrossRef.
  18. A. Das, J. P. Maher, J. A. McCleverty, J. A. N. Badiola and M. D. Ward, J. Chem. Soc., Dalton Trans., 1993, 681 RSC.
  19. A. C. T. North, D. C. Phillips and F. S. Matthews, Acta Crystallogr., Sect. A, 1968, 24, 351 CrossRef.
  20. A. Altomare, G. Cascarano, C. Giacovazzo, A. Guagliardi, G. Polidor, M. C. Burla and M. Camalli, J. Appl. Crystallogr., 1994, 27, 435 CrossRef.
  21. J. R. Carruthers and D. W. Watkin, Acta Crystallogr., Sect. A, 1979, 35, 698 CrossRef.
  22. A. C. Larson, Acta Crystallogr., 1967, 23, 664 CrossRef CAS.
  23. J. R. Carruthers and D. J. Watkin, CRYSTALS User Manual, Oxford University Computing Centre, Oxford, 1975 Search PubMed.
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