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DOI: 10.1039/A703834H (Paper) Reference Section for: Anal. Commun., 1997, 34, 201-204

Novel Ytterbium Complexes of Two Calix[4]resorcinarenes

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Sergey V. Shevchuk, Natalia V. Rusakova, Anna M. Turianskaya, Yurii V. Korovin, Ninel A. Nazarenko, Andrey I. Gren and Yurii E. Shapiro

Abstract

Calix[4]resorcinarenes, 2,8,14,20-tetramethyl- (L1 ) and 2,8,14,20-tetraphenyl- (L2) 5,11,17,23-tetradiethylamino- methylpentacyclo[19,3,1,13,7,19,13,115,19 ]octacosa- 1(25),3,5,7(26)9,11,13(27),15,17,19(28),21,23-dodecan- 4,6,10,12,16,18,22,24-octols, and their ytterbium complexes were synthesized. Some spectral-luminescence properties of Yb3+–L1 and Yb3+–L2 complexes were studied and their analytical possibilities were examined. The detection limit of ytterbium with L2 in YbCl3 solution was 0.09 µg ml-1.

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