N,N-Disubstituted alkanamides cleanly react with bis(trimethylsilyl)thioketene to form N,N-disubstituted 2-trimethylsilyl-3-trimethylsilyloxyalk-2-enethioamides, which upon acid hydrolysis give N,N-disubstituted 3-oxoalkenethioamides.
T. Tsuchiya, A. Oishi, I. Shibuya, Y. Taguchi and K. Honda, Chem. Commun., 1996, 1621 DOI: 10.1039/CC9960001621
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