A squre array of zirconium (IV) and iron(II) ions bound to a polyoxo matrix is achieved in the metallation of calix[4]resorcinarene (R = C6H13, H) using [Zr(η-C5H5)2Me2] and [Fe(phen)(mes)2], respectively.
E. Solari, W. Lesueur, A. Klose, K. Schenk, C. Floriani, A. Chiesi-Villa and C. Rizzoli, Chem. Commun., 1996, 807 DOI: 10.1039/CC9960000807
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