The crystal structures of U2V2O11 and UV2O8 have been determined using single-crystal X-ray and powder neutron diffraction. For U2V2O11, space group P21/n, a= 6.644(1)Å, b= 13.184(1)Å, c= 5.657(1)Å and β= 107.88(1)°, V= 471.59 Å3, Z= 2. For UV2O8, space group Pnma, a= 5.726(1)Å, b= 11.932(1)Å and c= 10.499(1)Å, V= 717.32 Å3, Z= 4. The structures are discussed in terms of linkages between UO7 and VO4 polyhedra.
A. M. Chippindale, P. G. Dickens, G. J. Flynn and G. P. Stuttard, J. Mater. Chem., 1995, 5, 141 DOI: 10.1039/JM9950500141
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