(+)-Nemorensic acid, the necic acid constituent of the pyrrolizidine alkaloid nemorensine, is shown to be (2R, 3R,5S)-2-carboxy-2,3,5-trimethyltetrahydrofuranacetic acid by synthesis from (R)-(+)-β-citronellol, and a corrected structure for the parent alkaloid nemorensine is established by a single crystal X-ray analysis.
M. P. Dillon, N. C. Lee, F. Stappenbeck and J. D. White, J. Chem. Soc., Chem. Commun., 1995, 1645 DOI: 10.1039/C39950001645
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