Using X-ray absorption fine structure measurements with a synchrotron source, the local environment of the titanium-centred active site of a siliceous mesoporous catalyst for the epoxidation of cyclohexane by H2O2 has been determined prior to the onset and during the course of catalysis.
G. Sankar, F. Rey, J. M. Thomas, G. N. Greaves, A. Corma, B. R. Dobson and A. J. Dent, J. Chem. Soc., Chem. Commun., 1994, 2279 DOI: 10.1039/C39940002279
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