Solution-phase electrochemical experiments involving free-solute species (here ferrocene) on macro-sized electrodes have been achieved on Pt at temperatures down to 99.5 K by use of an EtCl–THF–2-MeTHF–LiBF4 electrolyte.
S. J. Green, D. R. Rosseinsky and M. J. Toohey, J. Chem. Soc., Chem. Commun., 1994, 325 DOI: 10.1039/C39940000325
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