Selenoether macrocyclic chemistry: trans-[RhCl2([16]aneSe4)]BF4, synthesis, single crystal X-ray structure and 77Se NMR study ([16]aneSe4= 1,5,9,13-tetraselenacyclohexadecane)

Paul F. Kelly; William Levason; Gillian Reid; David J. Williams

doi:10.1039/C39930001716

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Selenoether macrocyclic chemistry: trans-[RhCl₂([16]aneSe₄)]BF₄, synthesis, single crystal X-ray structure and ⁷⁷Se NMR study ([16]aneSe₄= 1,5,9,13-tetraselenacyclohexadecane)

Paul F. Kelly, William Levason, Gillian Reid and David J. Williams

Abstract

trans-[RhCl₂([16]aneSe₄)]⁺, the first fully characterised example of a platinum metal selenoether macrocyclic complex, has been prepared in high yield; a single crystal X-ray structure determination on this complex is described together with its ⁷⁷Se NMR and electronic spectroscopic data.

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DOI: https://doi.org/10.1039/C39930001716
Article type: Paper

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J. Chem. Soc., Chem. Commun., 1993, 1716-1718

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Selenoether macrocyclic chemistry: trans-[RhCl₂([16]aneSe₄)]BF₄, synthesis, single crystal X-ray structure and ⁷⁷Se NMR study ([16]aneSe₄= 1,5,9,13-tetraselenacyclohexadecane)

P. F. Kelly, W. Levason, G. Reid and D. J. Williams, J. Chem. Soc., Chem. Commun., 1993, 1716 DOI: 10.1039/C39930001716

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Journal of the Chemical Society, Chemical Communications

Selenoether macrocyclic chemistry: trans-[RhCl₂([16]aneSe₄)]BF₄, synthesis, single crystal X-ray structure and ⁷⁷Se NMR study ([16]aneSe₄= 1,5,9,13-tetraselenacyclohexadecane)

Abstract

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Selenoether macrocyclic chemistry: trans-[RhCl₂([16]aneSe₄)]BF₄, synthesis, single crystal X-ray structure and ⁷⁷Se NMR study ([16]aneSe₄= 1,5,9,13-tetraselenacyclohexadecane)

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