A new method has been developed for the conversion of 1-nitrocycloalkenes to terminally unsaturated nitriles in one flask by use of Me3SiCH2MgCl (1.8 equiv.) and PCl3(2.5 equiv.) in tetrahydrofuran.
H. Tso, B. A. Gilbert and J. R. Hwu, J. Chem. Soc., Chem. Commun., 1993, 669 DOI: 10.1039/C39930000669
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