The reaction of the α-methoxylead derivative 1a with 2-phenylpropanal in the presence of TiCl4 gave the 1,2-syn-2,3-syn product 2 with very high diastereoselectivity: 1,2-syn/1,2-anti= 95/5 and 2,3-syn/2,3-anti= 100/0.
T. Furuta and Y. Yamamoto, J. Chem. Soc., Chem. Commun., 1992, 863 DOI: 10.1039/C39920000863
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