Issue 20, 1991
From the journal:

Journal of the Chemical Society, Chemical Communications

The reaction of coarse-grain metal powders with phosphoranes: a facile activation of metallic reagents and a novel route to metal–phosphine complexes. The X-ray crystal structures of Mnl2(PPhMe2) and FeBr3(PPhMe2)2

Stephen M. Godfrey,   David G. Kelly,   Anthony G. Mackie,   Philomena P. Mac Rory,   Charles A. McAuliffe,   Robin G. Pritchard  and  (the late)Susan M. Watson  

Abstract

A route to new and existing transition metal phosphine complexes is provided by the reaction of coarse-grain metal powders and phosphoranes in diethyl ether, as exemplified here by Nil3(PMe3)2, FeBr3(PPhMe2)2 and Mnl2(PPhMe2).

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Article information

DOI
https://doi.org/10.1039/C39910001447
Article type
Paper

J. Chem. Soc., Chem. Commun., 1991, 1447-1449

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The reaction of coarse-grain metal powders with phosphoranes: a facile activation of metallic reagents and a novel route to metal–phosphine complexes. The X-ray crystal structures of Mnl2(PPhMe2) and FeBr3(PPhMe2)2

S. M. Godfrey, D. G. Kelly, A. G. Mackie, P. P. M. Rory, C. A. McAuliffe, R. G. Pritchard and S. M. Watson, J. Chem. Soc., Chem. Commun., 1991, 1447 DOI: 10.1039/C39910001447

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