Facile dealkoxylation of aryl alkyl ethers has been carried out using TiCl3–Li–THF (tetrahydrofuran); a novel one-pot synthesis of phenanthrenes from ortho-alkoxyaromatic aldehydes/ketones is described.
A. Banerji and S. K. Nayak, J. Chem. Soc., Chem. Commun., 1991, 1432 DOI: 10.1039/C39910001432
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