A biphenomycin B analogue has been prepared using the double Heck coupling of 3,3′-diiodo-4,4′-dimethoxybiphenyl and two orthogonally protected 2-amidoacrylates followed by two peptide bond forming steps for the incorporation of L-lysine as the middle amino acid residue.
A. Carlström and T. Frejd, J. Chem. Soc., Chem. Commun., 1991, 1216 DOI: 10.1039/C39910001216
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