The dark-brown compound [N(Me)4]4[AsIII8VIV14O42(0.5H2O)] containing a spherical anion [AsIII8VIV14O42(0.5H2O)]4– containing condensed VO5 square pyramids and As 2O5 units, is synthesized hydrothermally from As2O3, V2O5 and (Me)4NOH and structurally characterized by X-ray diffraction.
G. Huan, M. A. Greaney and A. J. Jacobson, J. Chem. Soc., Chem. Commun., 1991, 260 DOI: 10.1039/C39910000260
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