Oxidation of 1,3-dithiane with different oxidizing agents gave the 1,3-dithiane cis- and trans-1,3-dioxides 1 and 2. Their configuration and the conformational preferences of the sulphinyl oxygen atom have been determined by NMR spectroscopy and by X-ray analyses.
S. Bien, S. K. Celebi and M. Kapon, J. Chem. Soc., Perkin Trans. 2, 1990, 1987 DOI: 10.1039/P29900001987
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