The structure of the unusual phenanthrene micandrol-C (7-methyl-1-methylthiophenanthrene-2,6-diol)(16), isolated from the trunkwood of the Amazonian tree, Micandropsis scleroxylon W. Rodr., is confirmed by synthesis. The key step involved the cyclization of a cis-2-chlorostilbene in the presence of activated magnesium.
M. V. Sargent and A. B. Zwicky, J. Chem. Soc., Perkin Trans. 1, 1990, 1713 DOI: 10.1039/P19900001713
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