EXAFS and 129Xe NMR data are presented which show that adsorption of Mo(CO)6 in zeolite NaY followed by decomposition at 200 °C produces uniformly dispersed Mo2 clusters in the zeolite supercages; heating to 400 °C causes sintering to an average cluster size of three or four Mo atoms.
J. M. Coddington, R. F. Howe, Y. Yong, K. Asakura and Y. Iwasawa, J. Chem. Soc., Faraday Trans., 1990, 86, 1015 DOI: 10.1039/FT9908601015
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