Anthracene adducts (4)–(6) are synthesized via a convenient general synthesis and subjected to a retro Diels-Alder reaction to furnish the corresponding 2-methylene-1,3-dioxygenated cyclopentenes and cyclopentanes (1)–(3)via either flash vacuum pyrolysis or room temperature silica gel-catalysed decomposition.
N. Chantarasiri, P. Dinprasert, C. Thebtaranonth, Y. Thebtaranonth and C. Yenjai, J. Chem. Soc., Chem. Commun., 1990, 286 DOI: 10.1039/C39900000286
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