Ultra-fine palladium particles (>2 nm diam.) which were well aged by electrochemical oxidation-reduction in an aqueous solution of HClO4 after being vacuum-evaporated on a flat plane of a glassy carbon electrode, have been observed by high resolution scanning electron microscopy (SEM).
Y. Takasu, K. Yahikozawa, N. Tateishi, M. Ueno and Y. Matsuda, J. Chem. Soc., Chem. Commun., 1990, 235 DOI: 10.1039/C39900000235
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